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Electroless Ni interlayer modified TiN coating by RF sputtering
Conference paper

Electroless Ni interlayer modified TiN coating by RF sputtering

J.G. Duh, J.C. Doong and C.T. Huang
American Society of Mechanical Engineers, Materials Division (Publication) MD, Vol.44, pp.209-215
1993

Abstract

An electroless nickel deposit is introduced as an interlayer between carbon steel substrate and r.f. magnetron sputtered TiN films, and a compound coating assembly TiN/Ni 3 P/Fe is derived after appropriate heat treatment. The employment of electroless Ni-P deposit results in an increase in the surface microhardness and the adhesion strength. The surface hardness as high as 2266 HK 1 close to the hardness of bulk TiN can be achieved in the Ni 3 P interlayer modified TiN coating. It is observed that the track depth after pin-on-disk test in TiN/Ni 3 P/Fe is about an order of magnitude small than that in the Fe substrate, and the introduction of electroless Ni interlayer in TiN coating provides a beneficial wear resistance. Corrosion behavior of the TiN coating assembly is evaluated through the polarization technique. The corrosion currents for TiN/Fe, Ni 3 P/Fe and TiN/Ni 3 P/Fe are 200, 40-70 and 5-7 μA/cm 2 , respectively. The presence of the electroless Ni-P interlayer in the modified TiN coating provides a better corrosion resistance as compared to conventional TiN coating on carbon steel.

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