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The nanoindentation characteristics of Cu6Sn5, Cu3Sn, and Ni3Sn4 intermetallic compounds in the solder bump
Conference paper   Peer reviewed

The nanoindentation characteristics of Cu6Sn5, Cu3Sn, and Ni3Sn4 intermetallic compounds in the solder bump

Guh-Yaw Jang, Jyh-Wei Lee and Jenq-Gong Duh
Journal of Electronic Materials, Vol.33(10), pp.1103-1110
10/2004

Abstract

Elastic modulus Hardness Intermetallic compound (IMC) Sn-Ag solder
In general, formation and growth of intermetallic compounds (IMCs) play a major role in the reliability of the solder joint in electronics packaging and assembly. The formation of Cu-Sn or Ni-Sn IMCs have been observed at the interface of Sn-rich solders reacted with Cu or Ni substrates. In this study, a nanoindentation technique was employed to investigate nanohardness and reduced elastic moduli of Cu <sub>6</sub> Sn <sub>5</sub> , Cu <sub>5</sub> Sn, and Ni <sub>3</sub> Sn <sub>4</sub> IMCs in the solder joints. The Sn-3.5Ag and Sn-37Pb solder pastes were placed on a Cu/Ti/Si substrate and Ni foil then annealed at 240°C to fabricate solder joints. In Sn-3.5Ag joints, the magnitude of the hardness of the IMCs was in the order Ni <sub>3</sub> Sn <sub>4</sub> > Cu <sub>6</sub> Sn <sub>5</sub> > Cu <sub>3</sub> Sn, and the elastic moduli of Cu <sub>6</sub> Sn <sub>5</sub> , Cu <sub>3</sub> Sn, and Ni <sub>3</sub> Sn <sub>4</sub> were 125 GPa, 136 GPa, and 142 GPa, respectively. In addition, the elastic modulus of the Cu <sub>6</sub> Sn <sub>5</sub> IMC in the Sn-37Pb joint was similar to that for the bulk Cu <sub>6</sub> Sn <sub>5</sub> specimen but less than that in the Sn-3.5Ag joint. This might be attributed to the strengthening effect of the dissolved Ag atoms in the Cu <sub>6</sub> Sn <sub>5</sub> IMC to enhance the elastic modulus in the Sn-3.5Ag/Cu joint.

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