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微脂粒藥物釋放系統界面性質之研究
Dissertation

微脂粒藥物釋放系統界面性質之研究

周宗翰
Doctor of Philosophy (PHD), 國立清華大學, 化學工程學系
2002

Abstract

微脂粒 混合單分子層 等溫線 壓縮係數 鬆弛行為 紫杉醇 界面性質 穩定性 liposomes mixed monolayers isotherm compressibility relaxation behavior paclitaxel interficial properties stability
This study is primarily concerned with the molecular interaction and the interfacial properties of mixed monolayers at the air/water interface at different temperatures. Measurement of surface pressure □□area per molecule (□□A) isotherms for DSPC/cholesterol, DSPC/DSPE-PEG2000, DSPC/paclitaxel, mixed monolayers, DSPC/cholesterol/DSPE-PEG2000 mixed monolayers, and DSPC/cholesterol/DSPE-PEG2000/paclitaxel mixed monolayers, respectively were conducted at different temperatures. Thermodynamic characteristics of these mixed systems at the air/water interface were studied from data obtained. The □□A isotherms showed these four components were miscible at 24.5℃. Temperature and compositions both had profound influence on the shape of isotherms, the compressibility, the stability, and the relaxation behavior of mixed monolayers. The most stable formulation can be determined by the estimation of the excess free energy of mixing. Additionally, the corresponding liposomal membrane stability of these mixed system was determined by release of encapsulated 5,6-carboxyfluorescein. Finally, the relevance of the observations for these mixed monolayers to the behavior in a liposomal domain was discussed.

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