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Fabrication of Porous Silicon Films by Electrochemical Etching and Its Application for Energy Storage Devices
Thesis

Fabrication of Porous Silicon Films by Electrochemical Etching and Its Application for Energy Storage Devices

Chang, Chih Tse
Masters, 國立清華大學, 材料科學工程學系
2014

Abstract

多孔矽 鋰離子電池 超級電容器 石墨烯 porous silicon lithium-ion battry supercapacitor graphene
This thesis aims to develop several processes of electrochemical etched porous silicon for either energy storage devices or demonstrating its potential for silicon-based solar cells. Silicon, the second most abundant material on earth, has been utilized in a wide range of regimes including batteries, semiconductor industry, and solar cells due to its low cost and well-developed technology. Porous silicon (PSi), as a functional material either due to its intrinsic property or the porous structure, has been presented to be fabricated by electrochemical etching, which is a facile and cost-effective method for producing porous silicon in a large scale. For lithium-ion batteries, the high theoretical capacity makes it a suitable candidate for anode material. However, the volume expansion during lithiation/delithiation limits its cycling performance. In this thesis, SiNPs produced from PSi has been exploited to lithium-ion batteries with excellent capacitance, columbic efficiency, and cycling retention. Porous silicon is further exploited as electrodes of supercapacitors after few-layer of graphene coating, showing competitive specific capacitance and stable cycling retention. In the last part of the results, porous silicon films and quasi-monocrystalline silicon films possessing extraordinary flexibility are exfoliated from silicon wafers, showing good potential for reusing the silicon wafers to reduce cost of Si-based solar cells.

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