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Optical and Electrical Properties of Vanadium Oxide Nanowires Synthesized by Thermal Evaporation Method
Thesis

Optical and Electrical Properties of Vanadium Oxide Nanowires Synthesized by Thermal Evaporation Method

Liu, Wei-Chang
Masters, 國立清華大學, 材料科學工程學系
2008

Abstract

氧化釩 熱蒸鍍法 奈米線 陰極發光光譜 電性 vanadium oxide thermal evaporation method nanowire CL spectrum electrical property
Vanadium dioxide (VO2) and divanadium pentoxide (V2O5) nanostructures have been synthesized by a thermal evaporation method. The growth follows vapor-solid (VS) growth mechanism. The electrical properties of VO2 nanowires and V2O5 nanowires and the cathodoluminescence (CL) of V2O5 nanowires were investigated. In the synthesis of stick-like VO2 nanostructures, argon was used as the carrier gas. Varying the growth temperatures can lead to different morphologies. The sizes of these structures are 100 nm - 5 □m in diameters and 3-10 □m in lengths. For V2O5 nanowires, the reaction proceeded under argon and oxygen atmospheres. The nanowires were grown on silicon, ITO-coated glass, and glass as the substrates. The growth temperature and heating time of ITO-coated glass substrate and glass substrate were different from the V2O5 nanowires on silicon substrate. The growth temperature of ITO-coated glass and glass substrate are lower than the silicon substrate. Prolonging the annealing time was found to play a role to decrease the defects in the V2O5 nanowires. The diameters and lengths of nanowires are 50-100 nm and 3-10 □m in lengths, respectively. Electrical properties of stick-like VO2 nanowire and V2O5 nanowire were measured. The resistivities of VO2 and V2O5 are 16.5 Ω-cm and 2.21 Ω-cm, respectively. The CL spectrum of V2O5 nanowires exhibits a green light emission peak at 550 nm corresponding to an energy gap of 2.3 eV.

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