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以DNA為模板之光還原金奈米粒子的表面增強拉曼散射感測器
Thesis

以DNA為模板之光還原金奈米粒子的表面增強拉曼散射感測器

戴鈞凱
Masters, 國立清華大學, 光電工程研究所
2013

Abstract

表面增強拉曼散射 DNA 光還原 Surface-Enhanced Raman Scattering DNA Photoinduced
In this work, we used the bio-organic polymer material full name (DNA), which has been widely employed in nanotechnology, in surface-enhanced Raman scattering (SERS) for biomedical sensing. A SERS substrate is presented to be used in sensing the interaction of alkaloid coralyne and DNA hybridization. We use the modified double helix DNA and weak photoreducing agent, Iragacure-2959, to synthesize rough surface flower-like gold nanostructures by photoreduction. By controlling the molar ratio of DNA, gold salt precursor and photoreducing agent, various morphologies and size of gold nanostructures can be obtained. We demonstrate the application of gold nanostructures as SERS substrate. The lowest detectable concentration of analytes, GM19 and DTNB is 10-9 M and the enhancement factor is 4.4×105 and 2.6×106, respectively. We apply this SERS substrate for sensors to detect the interaction of alkaloid coralyne and DNA. We determined the best combination ratio of coralyne and DNA by fluorescence spectroscopy. In addition, we also use the SERS intensity ratio (I736/I1318), which indicates the single-stranded and double-stranded DNA ratio, to verify coralyne concentration.

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