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以循環伏安法研究銅-胺基酸錯合物之電化學性質
Thesis

以循環伏安法研究銅-胺基酸錯合物之電化學性質

林景方
Masters, 國立清華大學, 生醫工程與環境科學系
2004

Abstract

銅-胺基酸錯合物 半可逆反應 非均相電子傳遞速率常數 量子產率
Abstract A detailed investigation on the electrochemical reduction of copper/amino acid complexes has been carried out using cyclic voltammetry with platinum microdisk electrode in aqueous solution containing 0.1M KCl as the supporting electrolyte. The stage of the first electron attachment is quasi-reversible reaction. The mechanism of the electrode process is following: We investigated the effects of nine different amino acids, that is α-alanine, asparagine, glutamine, glycine, isoleucine, proline, serine, threonine, valine on the rate constant of heterogeneous electron transfer, k0, of the quasi-reversible reaction of Cu(II)L2 calculated by the theory developed by Nicholson.The mean values of k0 with nine different amino acids were between 3.5×10-3 ~ 4×10-4 cm s-1 with a standard deviation of 45%.The order of k0 dose not have simple correlation with that of Cu(I) quantum yield at 313nm. Key words: Copper/amino acid complexes; quasi-reversible reaction; rate constant; heterogeneous electron transfer; quantum yield.

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