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以微波電漿化學氣相沉積低溫成長碳化矽
Thesis

以微波電漿化學氣相沉積低溫成長碳化矽

邱如謙
Masters, 國立清華大學, 材料科學工程學系
2012

Abstract

微波電漿化學氣相沉積 碳化矽 低溫 氯基 MICROWAVE PLASMA CVD PROCESS SIC LOW TEMPERATURE CHLORINE-BASED
We utilized the Microwave plasma enhanced chemical vapor deposition (MPECVD) as a non-heating process to grow 3C-SiC thin film, contained good crystal quality. We introduced Dichlorodimethylsilane (DDS) and Tetramethylsilane (TMS) into hydrogen plasma as reactant gases. Furthermore we compared how chlorine-based and chlorine-free precursor affects the process and results. We could obtain SiC thin film with good crystallinity at 400 ℃ with <111> preferred orientation and columnar-like structure on the sidewall of the film using chlorine-based process. Whereas, chlorine-free process showed more carbon aggregates in the grain boundary and lower crystallinity at similar process window. We referred the differences to the etching effect of SiCl2 which is believed to enhance the selective growth and suppress the secondary nucleation. Eventually we tried to deposit 3C-SiC on glass substrate to demonstrate the low process temperature feature and thus it can be used for optoelectric applications.

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