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以溶液方式製備萘苯亞醯胺衍生物作為n-type有機半導體材料
Thesis

以溶液方式製備萘苯亞醯胺衍生物作為n-type有機半導體材料

李亞蓮
Masters, 國立清華大學, 材料科學工程學系
2006

Abstract

萘苯亞醯胺 n-type有機半導體 旋轉塗佈法 有機電晶體 Naphthalene diimide n-type organic semiconductor spin-coating organic thin film transistor
This work is to synthesize new naphthalene diimide derivatives with different substituted side groups as organic semiconductor materials for future flexible electronic applications. Naphthalene diimide derivatives were spin-coated onto substrate via spin-coating process in air as semiconductor materials for OTFT fabrication using SiO2 or poly(vinyl- phenol) PVP as dielectrics. Electrical characteristics measurement and air-stability tests of OTFTs were carried out in air. For low-cost and low temperature process of organic thin film transistor (OTFT) applications, this work is mainly focused on developing new soluble, high air-stability semiconducting materials. The studies include improving solubility of organic semiconductor materials, fabricating OTFT devices via spin-coating process in air, and increasing organic semiconductor air-stability. Results show that three n-type organic material, 1,4,5,8- naphthalene-tetracarboxylic diimide derivatives material with alkyl, phenyl, and (trifluoro-methyl)-benzyl groups (NTCDI-C, NTCDI-P, and NTCDI-F) were successfully synthesized and deposited on a SiO2/Si or PVP/SiO2 wafer by the spin-coating process in air. The grain sizes of above NTCDI-derivatives thin films were 2-3 □m, 500-650 nm, and 300-400 nm, respectively. Transistor characteristics of OTFTs using NTCDI-derivatives as semiconductor layers were measured in air, with the motilities of about 10-3 cm2V-1s-1 for NTCDI-F and NTCDI-P. The NTCDI-F OTFTs also exhibit air-stability with only slight mobility degradation after exposure in air for 7 days. In a summary, a new solution-processed n-type semiconductor material, NTCDI-F, has been synthesized and investigated for OTFT fabrication via spin-coating process in air. Transistor characteristics and air-stability of OTFTs using NTCDI-F as semiconductor layers have been achieved. Results have demonstrated the feasibility of using solution-processed NTCDI-derivatives as semiconductors via spin- coating process in air for OTFT fabrication for future applications in flexible integrated circuits (ICs).

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