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以田口法最佳化多孔矽奈米粉末合成參數以改善鋰離子電池陽極材料充放電性質
Thesis

以田口法最佳化多孔矽奈米粉末合成參數以改善鋰離子電池陽極材料充放電性質

楊育碩
Masters, 國立清華大學, 材料科學工程學系
2013

Abstract

鋰離子電池 矽基陽極 田口法 多孔奈米材料
Energy storage system has become a critical technology for solving the oil crisis, and the lithium ion battery is one of the promising energy storage systems owing to the high theoretical energy and power density. Moreover, Silicon – based anode materials for lithium ion battery have been widely studied in recent years because the high specific capacities of silicon. This study uses Taguchi method to optimize the synthesis processes of porous silicon nanoparticles to improve the cycle life performance in lithium ion batteries. In the processes of SiO2 synthesis, there is a best ratio of CTACl / TEOS, 0.058, to form pores in nanoparticles, and a ratio of TOEA / TEA to form minimum particles. In the processes of Mg reduction, the best parameters for cycle life performance are: Outer pressure = 0.75 torr, Mg / SiO2 = 4, temperature = 625 oC, time = 6 hr. We conclude that the effect of porosity with large pore volume is less effective than that of particle size on the cycle life performance.

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