Abstract
This thesis is the report on the research work of crystal structure determination of eight compounds during my master degree study. It contained two parts: Part I. reviews the basic principle of X-ray structure determination; such as the relationship between Ewald sphere and Bragg’s law. Part II. comprises the eight crystal structures I solved. The structures are as following：Crystal 1. 1-(N,N-diethyl)-2-[2-(pyridyl) benzylidene] ethane triazido cobalt(III)Crystal 2. Bis-[1-ethyl-2-(p-tolylazo)] imidazole diazido copper(II)Crystal 3. 1,3-Bis[2-(pyridyl) benzylidene] propane azido copper(II) perchlorateCrystal 4. 1,4-Bis-[2-(pyridyl) benzylidene] butane diazido cadmium(II)Crystal 5. Bis-(μ-1,4-pyrazine)-diselenocyanate cadmium(II) PolymerCrystal 6. Bis[(4,4,-dipyridyl) disulfide]-bis[dicyano imide] diaquo manganese(II) (4,4,-dipyridyl) disulfideCrystal 7. 2,6-Bis(2-phenylazo) pyridineCrystal 8. 1,2-Bis(4-pyridyl) ethene monohydrate