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利用Rietveld method測定(La1-XNdX)0.7Sr0.3MnO3系統的結構並探討結構與磁性的關係
Thesis

利用Rietveld method測定(La1-XNdX)0.7Sr0.3MnO3系統的結構並探討結構與磁性的關係

陳炳元
Masters, 國立清華大學, 物理系
1998

Abstract

巨磁阻 鑭釹鍶錳氧 Rietveld 方法 X光粉末繞射 Colossal Magnetoresistance (La1-XNdX)0.7Sr0.3MnO3 Rietveld method X-ray powder diffractometry
A series of samples with nominal compositions of (La1-XNdX)0.7Sr0.3MnO3 (X = 0, 0.25, 0.5, 0.75, 1) system were prepared by solid state reaction process. The observation of "colossal" magnetoresistance (CMR) in these perovskite structural compounds has generated considerable interest in the physical properties of this class of compounds, particularly the interplay of structure, magnetism and electronic transport. It is believed that the CMR effect is due to a double exchange of electrons between ferromagnetically coupled Mn+3 and Mn+4 ions. Based on this reason, we have examined a series of samples, (La1-XNdX)0.7Sr0.3MnO3, Mn+3/Mn+4 ratio is fixed at 7/3. Powder X-ray diffraction method and Rietveld refinements were used to accomplish the structural analyses of these samples. With increasing X content, the structural symmetry changes from trigonal phase of (hexagonal axes, no.167) for X = 0, 0.25 to orthorhombic phase of Pnma (No.62) for X = 0.5, 0.75, 1. The lattice parameters a, b, c and angle of Mn-O-Mn are decreasing as X is increasing form 0 to 1. Magnetization and resistivity measurments indicate that the ferromagnetic-paramagnetic temperature Tc for these samples are almost the same as the metal-insulator temperature Tp and the largest magnetoresistance for each sample appeared around the temperature Tp. In addition, we observe that temperature Tc and Tp are decreasing as the Nd's content X is increasing.

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