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利用濕式環境穿透式電子顯微鏡臨場觀測二氧化鈦負載白金之光催化反應
Thesis

利用濕式環境穿透式電子顯微鏡臨場觀測二氧化鈦負載白金之光催化反應

黃慕若
Masters, 國立清華大學, 工程與系統科學系
2014

Abstract

穿透式電子顯微鏡 臨場光誘發分析 微型化濕室環境腔體 光纖導入光束系統 electron microscope in situ light-induced analysis wet cell fiber-based system
In this study, we design a “fiber-based system” which is using a UV light source with optical fiber to induce UV light through the EDS pole for JEM-2010. Because the TEM chamber must maintain at ultra-high vacuum environment, the sample can only in solid state. In order to observe wet sample in TEM, we use the wet-cell which is designed by our laboratory to prepare samples. Combine the fiber-based system with wet-cell technology let us having the chance to in-situ observes the photo-induced catalysis reaction in EM under nano-scale. We can confirm that the light-induced reaction is actually occurred under OM and TEM by the in-situ movies, difference in the images and the EDS analysis. The result makes sure that our home-make light induced system for TEM is workable.

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