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多壁奈米碳管/氧化鋁/環氧樹脂複合材料之製備與性質研究
Thesis

多壁奈米碳管/氧化鋁/環氧樹脂複合材料之製備與性質研究

蘇嬿如
Masters, 國立清華大學, 材料科學工程學系
2013

Abstract

奈米碳管 氧化鋁 環氧樹脂 電地暖 自加熱 CNT Al2O3 Epoxy electric floor heating self-heating Aluminium oxide
In this study, composites are made by epoxy as matrix to blend with the main fillers, Al2O3, as well as with the secondary fillers, mutli-walled carbon nanotubes (MWCNTs), at different ratios. Firstly, epoxy, CNTs and Al2O3 powders are evenly mixed by three-ball milling system to form adhesives. After degassing, the adhesives are cured at 140 oC for 3 h and pristine MWCNTs/Al2O3/epoxy composites are subsequently characterized by SEM and Raman. The glass transition temperature (Tg), mechanical, thermal and electrical properties are also measured, along with resistive heating experiments. The results show that comparing with pure epoxy, the specific heat of MWCNTs/Al2O3/Epoxy composite at 60 oC and 80 oC decrease 20 % (3-5 wt.% CNTs) and the thermal conductivity increase at least 300 % (1-5 wt.% CNTs) respectively. Input of low power (12-24 W) into composites (50×50×5 mm) produces heat and surface temperature reaches 60oC in 60-120 s and 80oC in 100-210 s respectively. Electrical heating of MWCNTs/Al2O3/Epoxy composites is low cost and is highly safety, capable of replacing existing electric floor heating systems.

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