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快速充電鋰離子二次電池負極複合碳材之研究
Thesis

快速充電鋰離子二次電池負極複合碳材之研究

李孟倫
Masters, National Tsing Hua University
2008

Abstract

鋰離子二次電池 Lithium ion battery
The electric vehicle (EV) is going to be one of the most important industries in this century, and the lithium-ion batteries should be the main choice of its power. High rate charging of lithium-ion battery is the major problem of this electric device. Recently, titanium-based compounds like spinel Li4Ti5O12 has become a popular anode material for the lithium ion battery, although it has a high-rate charging property but it also has a higher voltage plateau which is too high to an anode of general lithium ion batteries, and makes the application become narrow. MCMB (meso-carbon micro beads) is extended to be the anode material of the commercial lithium ion batteries for a long period of time, which is stable in voltage, capacity and cycle life performance, but without high-rate charging capability. In this study, we combine the advantages of these two materials, using the sol-gel process to modify the MCMB by coating Li4Ti5O12 to make a new material of Li4Ti5O12/MCMB composite anode. The phase of the produced Li4Ti5O12/MCMB composites particles was determined using powder x-ray diffraction (PXRD), and the grain size and morphology of the particle were examined through the field emission scanning electron microscope (FE-SEM). Some other tests are done for checking the electrochemical properties of the Li4Ti5O12/MCMB composites anode, it do shows the high-rate charging capability, while charging at 4C, the charging capacity is 160-170 mAh/g, and while charging at 6C, it still maintains the capacity over150 mAh/g. Under the charging rate of 0.05-6C, the Li4Ti5O12/MCMB composite anode can always show a flat voltage plateau at 0.3V, after several charging and discharging cycle, it still has a high-rate charging capability, and maintains a stable capacity. Finally, we use AC impedance and cyclic voltammetry analysis to test the oxidation and reduction of this material.

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