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新穎功能性高分子 Poly(Di(pyridin-2-yl)methyl acrylate) (PDPyMA) 的合成以及在異相催化反應的應用
Thesis

新穎功能性高分子 Poly(Di(pyridin-2-yl)methyl acrylate) (PDPyMA) 的合成以及在異相催化反應的應用

許毓容
Masters, 國立清華大學, 化學系
2014

Abstract

功能性高分子 異相催化劑 Suzuki-Miyaura 反應 醇氧化成醛與酮 Friedel-Crafts烷基化反應 Functional Polymer Heterogeneous Catalysts Suzuki-Miyaura Reactions Oxidation of Primary Alcohol to Aldehyde and Ketone Friedel-Crafts Alkylations
The multifunctional plateform of poly(di(pyridin-2-yl)methyl acrylate) (PDPyMA), which can coordinate with different metal ions to form the heterogeneous catalysts for various reactions, was obtained by the free radical polymerization of designed functional monomer of di(pyridin-2-yl)methyl acrylate (DPyMA). The insoluble powders formed from PDPyMA and metal salts like Pd(OAc)2 and Cu(OTf)2 have been used to catalyze different reactions such as oxidation of primary alcohol to aldehyde and ketone, Suzuki-Miyaura reactions, and Friedel-Crafts alkylations. The performance of these heterogeneous catalysts was similar or only slightly lower than the soluble monomeric complexes that formed by DPyMA and corresponding metal salts, indicating that the steric hindrance caused by polymeric plateform was not significant. The catalysts based on PDPyMA were recycled by simple filtration and rinse with no observable weight loss nor activity decline.

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