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於鈦金屬上合成二氧化鈦奈米結構應用於無連結劑之鋰離子電池陽極
Thesis

於鈦金屬上合成二氧化鈦奈米結構應用於無連結劑之鋰離子電池陽極

潘玠城
Masters, 國立清華大學, 材料科學工程學系
2014

Abstract

二氧化鈦 奈米線 奈米片 奈米板 鋰離子電池陽極 Titanium dioxide nanowire lithium ion batteries anode
In our work, anatase TiO2 nanostructures on Ti foil transformed from sodium titanate were synthesized by a facile hydrothermal reaction. Under different hydrothermal conditions, diverse morphologies including nanowire, nanosheet and nanobelt can be obtained. The rate of sodium ion intercalating into TiO6 structure during the hydrothermal reaction will influence the morphology of sodium titanate. High intercalation rate occurring at high temperature and high sodium ion concentration environment leads to the formation of nanowire TiO2. On the contrary, lamellar TiO2 including nanosheet and nanobelt were obtained in low intercalation rate condition. Anatase TiO2 on conductive Ti foil can be used as a binder-free anode material for lithium ion batteries. Nanowire exhibits the best lithium ion batteries performance among three different morphologies and retains 220.95 mAh/g after 100 cycles at the rate of 1 C (335 mA/g). In variable current test, at the rate of 20 C (6.7 A/g), anatase TiO2 nanowire still remains 99.04 mAh/g. The extraordinary performance can be attributed to high specific surface area and low charge transfer resistance. This result suggests that anatase TiO2 growing on Ti foil can be a promising candidate for high performance lithium ion batteries.

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