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樟腦衍生之胺化合物催化二羥基丙酮與醛類衍生物進行不對稱醛醇反應
Thesis

樟腦衍生之胺化合物催化二羥基丙酮與醛類衍生物進行不對稱醛醇反應

林佳誼
Masters, 國立清華大學, 化學系所
2016

Abstract

不對稱催化 醛醇反應 Asymmetric catalysis Aldol reaction
This thesis dealt with the use of dihydroxyacetone as a C3 donor with 4-nitrobenzaldehyde in the asymmetric aldol reaction catalyzed by amines as organocatalyst. The effect of solvent, temperature, additive and mole ratio of reactants were studied. It was found that in the presence of 20 mol% catalyst 27 and 20 mol% benzoic acid additive in the DCM-propionitrile (7/1) mixed solvent system, afforded syn aldol product in 42% yield, moderate diastereoselevtivity (1:6.5) and good enantioselectivity (84%).

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