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直接影像觀察與X光光電子影像分析鈣鈦礦 碘離子在電場下之遷移現象
Thesis

直接影像觀察與X光光電子影像分析鈣鈦礦 碘離子在電場下之遷移現象

張庭偉
Masters, 國立清華大學, 化學系所
2016

Abstract

鈣鈦礦 離子遷移 perovskite ion migration
In this thesis, we will report on an investigation of how the organo-halide perovskite solar cell, thin-film materials of varied halide content, MAPbI3, MAPbI2Br, MAPbIBr2, MAPbBr3, behave under the applied electrical field and under different controlled environments of dry and moist nitrogen atmosphere. The morphology of the film of different length scale was examined with optical microscope (OM) and atomic force microscope (AFM). The chemical composition of the films was measured with X-ray photoemission spectroscopy (XPS) with particular emphasis given to I 3d, Pb 4f, and Br 3d because of the known migration of ionic species that is enhanced under the influence of electrical field and accelerated decomposition in moist environment. One dimensional XPS imaging was also used to map out the distribution of ionic species across the electrodes. Our results show that the iodide migration among four types of perovskite films, as vividly demonstrated with moving traces in OM, varies with the I/Br ratio and the environment where the electrical field was applied. Higher bromide content and dry environment can significantly retard the halide migration, due to the enhanced stability contributed by bromide ions.

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