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鐵鈀銦及鐵鈀金鐵磁性形狀記憶合金均質化處理之研究
Thesis

鐵鈀銦及鐵鈀金鐵磁性形狀記憶合金均質化處理之研究

羅元宏
Masters, National Tsing Hua University
2008

Abstract

鐵磁性形狀記憶薄帶均質化 FerromagneticShape MemoryRibbonHomogenization
In this study the effect of cold rolling and homogenization on the transformation temperature, magnetization, magnetostriction and shape memory effect for melt-spun FePd29.5In0.5 and FePd30-xAux (x = 1, 5 and 7) alloys were investigated. The homogenized FePd29.5In0.5 ribbon exhibited complete bct phase while only little bct was observed in the as-spin ribbon, on the other hand, no bct phase was observed in both as-spun and homogenized FePd30-xAux ribbons (x = 1, 5 and 7). The Ms of homogenized FePd30-xAux was found to decrease with Au content, while the Af of as-spun FePd30-xAux increased with Au content. At room temperature FePd23Au7 exhibited complete parent phase. As-spun FePd29.5In0.5 ribbon exhibited higher room temperature saturated magnetization than that of homogenized sample, while the coercive field of the latter is lower. For as-spun and homogenized FePd30-xAux ribbon the room temperature saturated magnetization decreased with increased Au content. The magnetostriction of as-spun FePd29.5In0.5 reached maximum at 375 ppm under 9 kOe at 80° with respect to the field, and that of homogenized sample reached maximum at 415 ppm at 70° under 9 kOe. Homogenized FePd30-xAux exhibited higher magnetostriction under 9 KOe field, and the values are 1240 ppm at 90°, 1330 ppm at 80° and 760 ppm at 90° for X = 1, 5 and 7 respectively. As-spun FePd29.5In0.5 exhibited Two-way shape memory effect with recovery ratio up to 35% after 50 thermal cycles, while the homogenized ribbon showed no shape memory effect due to the BCT phase. For homogenized FePd30-xAux the recovery ratio was only up to 10% after 50 thermal cycles while that of as-spun ribbon exhibited much higher recovery ratio up to 58% for X=7.

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