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開發氣相電分離法分析膠體奈米銀粒子於配方化學中穩定性變化之研究
Thesis

開發氣相電分離法分析膠體奈米銀粒子於配方化學中穩定性變化之研究

戴睿霆
Masters, 國立清華大學, 化學工程學系
2014

Abstract

奈米銀粒子 膠體穩定性 電噴灑式氣相奈米粒子流動分析儀 silver nanoparticle colloidal stability electrospray-differential mobility analysis
Silver nanoparticle (AgNP) is widely used in our daily life, including consumer goods, clothes, electronics, and also many emerging technology in biomedical applications (e.g., carriers, sensors). In this study, we investigated the colloidal stability of AgNPs under acidic and/or highly ionic environments, and the subsequent interaction with the plasma protein to their colloidal stability. Electrospray-differential mobility analysis was used to characterize the particle size distributions and the number concentrations of AgNPs. Transmission electron microscopy was employed orthogonally to provide visualization of AgNPs. For unconjugated AgNPs, the particles size was increased by aggregation as increasing the acidity and/or ionic strength, accompanied with a change of morphology due to acid-induced interfacial dissolution, but aggregation and dissolution were both shown to be insignificant for bovine serum albumin-functionalized AgNPs. This work provides a generic method to analyze colloidal stability of surface functionalized AgNPs over various formulation chemistry and environment conditions (e.g., cell culture media and natural water).

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