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非等莫耳六元CoFeMnTiVxZry (0.4 ? x, y ? 3)高熵合金之儲氫研究
Thesis

非等莫耳六元CoFeMnTiVxZry (0.4 ? x, y ? 3)高熵合金之儲氫研究

許臻豪
Masters, National Tsing Hua University
2007

Abstract

等莫耳與非等莫耳高熵合金壓力成分等溫曲線Laves相CoFeMnTiVxZry平均分配法計算結合焓 equal- and non-equal-molar high-entropy alloysPCI curvesLaves phaseCoFeMnTiVxZryequipartition method for formation enthalpy calculation
Storage capacity, working pressure and temperature, cycle life, and rate of absorption and desorption in hydrogen storage are current emphasized developing issues. We use a vacuum arc remelter to prepare as-cast alloys. The alloys are characterized by scanning electron microscopy (SEM), energy-dispersive x-ray spectroscopy (EDS), and x-ray diffractometry (XRD). Pressure-composition-isotherm (PCI) curves are used to investigate the absorption and desorption of hydrogen. After detailed investigation we conclude that both equal- and non-equal-molar high-entropy alloys have a high potentiality in hydrogen storage.Results on Laves phase-related CoFeMnTiVxZry (0.4 ≦ x, y ≦ 3) high-entropy alloys shows that with Zr as a component, high-entropy alloys are easily activated and absorb hydrogen. Simultaneous addition of Zr and V improves the capacity of hydrogen absorption. In this experiment, we first adopt the most popularly used equal-molar compositions in high-entropy alloys as a base to find a suitable alloy series, then change the relative amount among components in alloys or make substitution for elements to investigate in detail the effects of elements and non-equal molar compositions on the hydrogen storage properties.An equipartition method (EPM) for calculation formation enthalpy of multicomponent metal hydrides proposed in this study shows a linear relationship between enthalpy per mole atom in alloy and maximum storage capacity in atomic ratio for a single system. On the other hand, for different systems total energy determines the maximum storage capacity among systems.

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