Logo image
Characterization of the Effects of Vanadium Traps in Cracking Catalysts by Imaging Secondary Ion Mass Spectrometry and Microactivity Test
Journal article   Peer reviewed

Characterization of the Effects of Vanadium Traps in Cracking Catalysts by Imaging Secondary Ion Mass Spectrometry and Microactivity Test

Long-Hui Lin, Kuei-Jung Chao, Yong-Chien Ling, Jan-Fu Hwang and Liang-Yuan Hou
Journal of the Chinese Chemical Society, Vol.44(6), pp.553-558
1997

Abstract

Microactivity test SIMS Vanadium trapping in cracking catalysts
The vanadium trapping effect of Mg and La containing additives in cracking catalyst contaminated with 2300 ppm Ni and 4700 ppm V has been analyzed by microactivity test (MAT) and imaging secondary ion mass spectrometry (SIMS). The results of SIMS imaging are consistent with cracking activity data and show that the La/spinel is a superior vanadium trap for the fluid catalytic cracking of hydrocarbons (FCC) operation La/spinel serves as a dual function additive for both vanadium trap and SO x removal. The optimum amount of La/spinel added to the cracking catalyst is about 15% by weight. This results in an increased catalytic activity, an increase in gasoline yield, and a decrease in coke and gas factors. The MgAl 2 O 4 phase of Mg/Al 2 O 3 additive is found capable of trapping vanadium while its MgO of Mg/Al 2 O 3 phase can migrate to zeolite particles (the active component of the FCC catalyst) that, in turn, causes a decline in the activity of that catalyst.

Metrics

1 Record Views

Details

Logo image