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Crystallization and melting behavior of poly(ε-caprolactone) under physical confinement
Journal article   Peer reviewed

Crystallization and melting behavior of poly(ε-caprolactone) under physical confinement

Rong-Ming Ho, Yeo-Wan Chiang, Chu-Chien Lin and Bor-Han Huang
Macromolecules, Vol.38(11), pp.4769-4779
31/05/2005

Abstract

The crystallization and melting behavior of Poly(εcaprolactone) (PCL), were studied in a physically confined system using differential scanning calorimetry (DSC). Macrophase-separation and macro-phase separated morphology were identified in the self-assembly blends. The crystallization rate of PCL was found to be strongly affected by the phase-separated morphology, and the effective confinement on crystallization occured while the size of lamellae-like confinement goes below submicrometer. Recognizable melting depression was found for PCL under confinement, whereas significant decrease on relative crystallinity was observed for PCL chains crystallized at higher temperature.

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