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(Dithio-benzoato-κ2 S,S′)[hydridotris(pyrazol-1-yl-N κ2)borato](triphenyl-phosphine-P)ruthenium(II)
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(Dithio-benzoato-κ2 S,S′)[hydridotris(pyrazol-1-yl-N κ2)borato](triphenyl-phosphine-P)ruthenium(II)

Chia-Her Lin, Yao-Ren Liang, Hung-Chun Tong, Yih Hsing LoTing Shen Kuo
Acta Crystallographica Section E: Structure Reports Online, 卷.64(12)
2008

摘要

Chemistry (all) Materials Science (all) Condensed Matter Physics
Reaction of [Ru(Tp)Cl(PPh3)2] (Tp = hydridotrispyrazolyl-borate) with ammonium dithio-benzoate in methanol leads to the formation of the title compound, [Ru(C9H10BN6)(C7H5S2)(C18H15P)]. In the crystal structure, the Ru atom is coordinated by three N atoms of the Tp ligand, one P atom of the triphenyl-phosphine ligand and the two S atoms of the dithio-benzoate ligand within a slightly distorted octa-hedron. The Ru - S bonds are slightly different [2.321 (1) and 2.396 (1) Å] and the average N - Ru - N angle is 86.31°. © 2008.

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https://doi.org/10.1107/S1600536808036702檢視
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