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Facile synthesis of 2,5-diarylthiazoles via palladium-catalyzed tandem C-H substitutions. Design of tunable light emission and liquid crystalline characteristics
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Facile synthesis of 2,5-diarylthiazoles via palladium-catalyzed tandem C-H substitutions. Design of tunable light emission and liquid crystalline characteristics

Atsunori Mori, Akitoshi Sekiguchi, Kentaro Masui, Tomohiro Shimada, Masaki Horie, Kohtaro Osakada, Masuki KawamotoTomiki Ikeda
Journal of the American Chemical Society, 卷.125(7), 頁碼.1700-1701
15/02/2003

摘要

A mild and regioselective C-H substitution reaction of thiazole by the catalysis of the palladium/copper system is found to proceed in the presence of tetrabutylammonium fluoride under mild conditions. Applying the new reaction, we synthesized various 2,5-diarylthiazoles that exhibit light-emitting and liquid crystalline characteristics in good yields. The color of light emission is tunable by the introduction of the substituent. Differently substituted 2,5-diarylthiazoles are found to exhibit a stable liquid crystal phase in a wide temperature range. Copyright © 2003 American Chemical Society.

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