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Ferroelectric properties of Pb(Zr1-x,Tix)O 3 prepared by modified metallo-organic-decomposition process
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Ferroelectric properties of Pb(Zr1-x,Tix)O 3 prepared by modified metallo-organic-decomposition process

Shih-Yen Liu, Chen-Shan Chou, Jin-Hua HuangI.-Nan Lin
Integrated Ferroelectrics, 卷.52, 頁碼.11-18
2003

摘要

Ferroelectric properties MOD Nano-powder PZT Control and Systems Engineering Electronic Optical and Magnetic Materials Ceramics and Composites Condensed Matter Physics Materials Chemistry Electrical and Electronic Engineering
Beneficial effect of nano-sized PZT powder incorporation on modifying the characteristics of Pb(Zr 0.52 Ti 0.48 )O 3 , PZT films was demonstrated. The amorphous phase derived from metallo-organic- decomposition (MOD) process started to crystallize at a post-annealing temperature as low as 500°C and can withstand 650°C post-annealing temperature process without inducing the PbO-loss phenomenon. However, 500°C post-annealed PZT films still exhibit paraelectric properties, which can be ascribed to the co-existence of large proportion of amorphous phase, surrounding the crystalline phase. It needs at least 650°C post-annealing process to fully developed the pervoskite structure for PZT films. The remnant polarization (Pr) of the PZT films increases with the proportion of crystalline phase, achieving Pr = 24.9 μC/cm 2 for 650°C annealed films, with coercive field (Hc) around Ec = 373 kV/cm.

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