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Gelation and degelation of PVA in aqueous BaTiO3 slurries
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Gelation and degelation of PVA in aqueous BaTiO3 slurries

Chia-Chen LiChung-Hsuan Chang
Journal of the American Ceramic Society, 卷.96(2), 頁碼.436-441
02/2013

摘要

Ceramics and Composites Materials Chemistry
Poly(vinyl alcohol) (PVA) gels favorably with boron oxide (B 2 O 3 ) in aqueous slurries of BaTiO 3 , resulting in a dilatant rheology, but the gelation and dilatancy can be efficiently reduced by the use of hydroxylated BaTiO 3 . The degelation effect caused by the use of hydroxylated BaTiO 3 was studied, and the corresponding degelation mechanisms were clarified. Interestingly, the hydroxylated BaTiO 3 interacts better than the as-received form with PVA and B 2 O 3 , and the hydroxylated form is more chemically stable and less soluble in the aqueous slurry. Based on these specific properties of hydroxylated BaTiO 3 , especially its good chemical stability, the free concentrations of PVA and - B(OH) 4 in the aqueous slurry are efficiently diminished. The decreased free concentrations of PVA and B 2 O 3 facilitate the reduction of the gelation opportunity between them, leading to a great improvement in the rheological behavior of the aqueous slurries. © 2013 The American Ceramic Society.

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