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Gold- and silver-catalyzed [4+2]cycloadditions of ynamides with oxetanes and azetidines
Journal article   Peer reviewed

Gold- and silver-catalyzed [4+2]cycloadditions of ynamides with oxetanes and azetidines

Samir Kundlik Pawar, Dhananjayan Vasu and Rai-Shung Liu
Advanced Synthesis and Catalysis, Vol.356(11-12), pp.2411-2416
11/08/2014

Abstract

2-amino-1,4,5,6-tetrahydropyridines 6-amino-3,4-dihydro-2H-pyrans azetidines gold(I) and silver(I) catalysis oxetanes ynamides
Gold-catalyzed [4+2]cycloadditions between ynamides and oxetanes are described; these reactions involve oxetanes and gold-π-ynamides as nucleophiles and electrophiles, respectively. Excellent cycloaddition regioselectivities are achieved over a reasonable range of ynamide and oxetane substrates. For azetidines, their [4+2]cycloadditions with ynamides are implemented more efficiently with silver hexafluoroantimonate, which is also compatible with various ynamides and azetidines. These two cycloadditions provide facile accesses to six-membered heterocycles such as 6-amino-3,4-dihydro-2H-pyrans and 2-amino-1,4,5,6-tetrahydropyridines. © 2014 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim.

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