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Gold-Catalyzed Bicyclic Annulations of N-(o-Alkynylphenyl)imines with α-Diazo Esters to Form 5,6-Dihydroindolo[2,1-A]isoquinolines
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Gold-Catalyzed Bicyclic Annulations of N-(o-Alkynylphenyl)imines with α-Diazo Esters to Form 5,6-Dihydroindolo[2,1-A]isoquinolines

Akshay Subhash NarodeRai-Shung Liu
Organic Letters, 卷.24(11), 頁碼.2165-2169
03/2022
PMID: 35285228

摘要

Biochemistry Physical and Theoretical Chemistry Organic Chemistry
One-pot synthesis of 5,6-dihydroindolo[2,1-A]isoquinolines from gold-catalyzed annulations between N-(o-Alkynylphenyl)imines and α-diazo esters is described. This cascade reaction involves an initial attack of the diazo ester at the imine to form cis-Aziridine, followed by stereoselective [3 + 3]-Annulations with the tethered arylalkyne. We have employed this new catalysis to prepare one bioactive 5,6-dihydroindolo[2,1-A]isoquinoline molecule.

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