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Microhardness of sputtered ternary Ni-P-W coating with extra-high phosphorous content from improved deposition rate-derived electroplated NiP targets
Journal article   Open access   Peer reviewed

Microhardness of sputtered ternary Ni-P-W coating with extra-high phosphorous content from improved deposition rate-derived electroplated NiP targets

Chih-Hsiung Lin and Jenq-Gong Duh
Surface and Coatings Technology, Vol.188-189(1-3 SPEC.ISS.), pp.495-499
11/2004

Abstract

Electroplating Microhardness Ni-P-W deposit R.f. sputtering Sputtered Ni-P
The ternary Ni-P-W alloy coating was fabricated by RF magnetron sputtering technique with dual targets of Ni-P/Cu and pure W. Electroplating Ni-P process was introduced to obtain the NiP compound target with extra-high phosphorous contents around 21 at.%. The deposition rate achieved as high as 20 μm/h after modification of the processing parameters. The Ni-P-W coating with a high P/Ni ratio of 0.25 was successfully derived by electroplating with a high P content Ni-P/Cu target. After heat treatment, the coating was strengthened by the precipitation of Ni-P compounds and solutioning of W in the crystallized Ni matrix. The Ni-P-W coating exhibited a relatively higher hardness with higher P codeposited after annealing at elevated temperature. The advantage of the composite target was also discussed by comparing with the ternary deposit fabricated by the electroless process. © 2004 Elsevier B.V. All rights reserved.
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