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Pressure-induced structural distortion of TbMnO3: A combined x-ray diffraction and x-ray absorption spectroscopy study
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Pressure-induced structural distortion of TbMnO3: A combined x-ray diffraction and x-ray absorption spectroscopy study

J.M. Chen, T.L. Chou, J.M. Lee, S.A. Chen, T.S. Chan, T.H. Chen, K.T. Lu, W.T. Chuang, H.-S. Sheu, S.W. Chen, …
Physical Review B - Condensed Matter and Materials Physics, 卷.79(16), 165110
04/2009

摘要

Electronic Optical and Magnetic Materials Condensed Matter Physics
The variation of electronic states and structural distortion in highly compressed multiferroic TbMnO3 was probed by x-ray diffraction (XRD) and x-ray absorption spectroscopy (XAS) using synchrotron radiation. Refined XRD data enabled observation of a reduced local Jahn-Teller (JT) distortion of Mn sites within MnO6 octahedra in TbMnO3 with increasing hydrostatic pressure. A progressively increasing intensity of the white line in MnK -edge x-ray absorption spectra of TbMnO3 was detected with increasing pressure. The absorption threshold of MnK -edge spectra of TbMnO3 is shifted toward higher energy, whereas the pre-edge peak is slightly shifted to lower energy with increasing hydrostatic pressure. We provide spectral evidence for pressure-induced bandwidth broadening for mangnites. The enhanced intensity of the white line and the shifted absorption threshold of MnK -edge spectra are explained in terms of a reduced JT distortion of MnO6 octahedra in compressed TbMnO3. Comparison of XAS data with full-multiple-scattering calculations using code FDMNES shows satisfactory agreement between experimental and calculated MnK -edge spectra. © 2009 The American Physical Society.

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