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Synthesis and X-ray structures of cyclometalated iridium complexes including the hydrides
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Synthesis and X-ray structures of cyclometalated iridium complexes including the hydrides

Chao Wang, Hsin-Yi Tiffany Chen, John Bacsa, C. Richard A. CatlowJianliang Xiao
Dalton Transactions, 卷.42(4), 頁碼.935-940
01/2013
PMID: 23086557

摘要

Inorganic Chemistry
Cyclometalation of [Cp*IrCl 2 ] 2 with ketimine ligands generated very active catalysts for transfer hydrogenation of imines as well as reductive amination. The synthesis and X-ray diffraction structures of three such complexes are disclosed in this paper. The hydrides of two complexes, key intermediates in hydrogenation, have been isolated and their structures determined by X-ray diffraction as well. © The Royal Society of Chemistry 2013.

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