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Synthesis, characterization, and properties of photosensitive silicon-containing copolyimides
Journal article   Peer reviewed

Synthesis, characterization, and properties of photosensitive silicon-containing copolyimides

YU-DER LEE, Chi Chi Lu and Hurng Rern Lee
Journal of Applied Polymer Science, Vol.41(3-4), pp.877-888
1990

Abstract

Copolyimides with siloxane moieties in the main chain were synthesized by solution polycondensation of 1,3-bis (3-aminopropyl) tetramethyldisiloxane (APMS), oxydianiline (ODA) with 3,3′,4,4′-benzophenone tetracarboxylic dianhydride (BTDA) in N-methyl-2-pyrrolidone (NMP). The adhesion properties between copolyimides and silicon wafer were improved significantly with incorporation of siloxane moiety into polymer chain. Photosensitive copolyimide precursor was obtained by further reaction of silicon-containing copolyamic acid with 2-isocyanatoethyl methacrylate (IEM).

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