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The stability of γ′ precipitates in a multi-component FeCoNiCrTi0.2 alloy under elevated-temperature irradiation
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The stability of γ′ precipitates in a multi-component FeCoNiCrTi0.2 alloy under elevated-temperature irradiation

Guma Yeli, Da Chen, Kiyohiro Yabuuchi, Akihiko Kimura, Shaofei Liu, Weitong Lin, Yilu Zhao, Shijun ZhaoJi-Jung Kai
Journal of Nuclear Materials, 卷.540, 152364
11/2020

摘要

Atom probe tomography Disordering and dissolution High-entropy alloys Ion irradiation γ′ precipitates Nuclear and High Energy Physics Materials Science (all) Nuclear Energy and Engineering
Precipitation hardening by γ′ precipitates is an effective strengthening mechanism for designing novel high-entropy alloys (HEAs). The stability of these γ′ precipitates under elevated temperature irradiation is a major concern for their application in nuclear industry. In the present study, a γ′-strengthened FeCoNiCrTi 0.2 HEA is irradiated using 6.4 MeV Fe 3+ ions at 400 °C, 500 °C and 600 °C, respectively. After irradiation, transmission electron microscopy (TEM) and atom probe tomography (APT) has characterized the structural and compositional stability of the γ′ precipitates. The results show that the ordered L1 2 structure of γ′ precipitate is susceptible to the radiation damage, whereas their basic compositional features can sustain up to ∼13 dpa at these temperatures. APT reveals that the dissolution of γ′ precipitates start from the surface of the precipitates at the early stage of irradiation. Dissolution and disordering of the precipitates are dependent on the irradiation dose and temperature. APT also shows that small Ni and Ti-rich clusters form after irradiation at elevated temperatures. The behavior of γ′ precipitates under irradiation is believed to be controlled by two competing factors, displacement damage and radiation enhanced diffusion. Both can influence the radiation induced disordering/dissolution and reprecipitation.

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