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Total synthesis of an immunomodulatory phosphoglycolipid from thermophilic bacteria
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Total synthesis of an immunomodulatory phosphoglycolipid from thermophilic bacteria

Hong-Jyune Lin, Avijit Kumar Adak, L. Vijaya Raghava Reddy, Shih-Hsiung WuChun-Cheng Lin
Chemistry - A European Journal, 卷.19(24), 頁碼.7989-7998
06/2013
PMID: 23595956

摘要

diastereoselectivity glycolipids glycosylation immunomodulators phosphoglycolipids total synthesis Chemistry (all)
A method for the stereocontrolled synthesis of a bacterial phosphoglycolipid (PGL1) isolated from thermophilic bacteria is described. The key features of the synthesis include a highly α-selective glycosylation reaction between a trichloroacetimidate donor and a D-lyxose-derived primary alcohol acceptor and the late-stage incorporation of the phospholipid. Copyright © 2013 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim.

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