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Using poly(4-styrene sulfonic acid) to improve the dispersion homogeneity of aqueous-processed LiFePO4 cathodes
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Using poly(4-styrene sulfonic acid) to improve the dispersion homogeneity of aqueous-processed LiFePO4 cathodes

Chia-Chen Li, Xing-Wei Peng, Jyh-Tsung LeeFu-Ming Wang
Journal of the Electrochemical Society, 卷.157(4)
2010

摘要

Electronic Optical and Magnetic Materials Renewable Energy Sustainability and the Environment Surfaces Coatings and Films Electrochemistry Materials Chemistry
The dispersion properties of aqueous lithium iron phosphate (LiFePO 4 ) slurries and the electrochemical properties of the corresponding as-prepared cathodes with the addition of a dispersant, poly(4-styrene sulfonic acid) (PSSA), have been investigated. The influence of PSSA on the dispersion behaviors of LiFePO 4 and conductive agents, graphite and carbon black, in aqueous suspensions are explored by the analyses of zeta-potential and rheology. The results show that the PSSA adsorbs onto the LiFePO 4 and conductive agents so that they can be electrosterically stabilized in aqueous suspensions. Through the observation using a scanning electron microscope, it is shown that the homogeneity and dispersion of the composition distributed in the LiFePO 4 electrode sheet are significantly improved with increasing content of PSSA. However, an excess addition of PSSA is detrimental to the electronic conduction and the electrical capacity of the cathode. To obtain a homogeneous electrode with a good cell performance, the optima content of PSSA is suggested to be 2.0 wt % based on the LiFePO 4 weight. © 2010 The Electrochemical Society.

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